N′-(2-Fluoro­benzyl­idene)acetohydrazide

نویسندگان

  • Jie Yang
  • Zhao-De Jiang
  • Fu-Gong Zhang
  • Fang-Fang Jian
چکیده

The title compound, C(9)H(9)FN(2)O, was prepared by the reaction between 2-fluoro-benzophenone and acetohydrazide. In the crystal structure, inversion dimers linked by pairs of N-H⋯O hydrogen bonds occur, generating R(2) (2)(8) loops.

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منابع مشابه

N′-(4-Fluoro­benzyl­idene)acetohydrazide

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N′-(4-Fluoro­benzyl­idene)-2-(4-fluoro­phen­yl)acetohydrazide

In the title compound, C(15)H(12)F(2)N(2)O, the dihedral angle between the two benzene rings is 48.73 (8)°. The hydrazine group is twisted slightly, with a C-N-N-C torsion angle of 172.48 (12)°. In the crystal, mol-ecules are connected by strong N-H⋯O and weak C-H⋯O hydrogen bonds, forming supra-molecular chains along the c axis. The structure is consolidated by π-π [centroid-centroid separatio...

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In the title compound, C(8)H(9)ClN(2)O(2), the acetohydrazide group is approximately planar, with the maximum deviation of 0.031 (2) Å. In the crystal, the mol-ecules are linked by N-H⋯N, N-H⋯O and C-H⋯O hydrogen bonds, with the acetohydrazide O atom accepting two C-H⋯O links and one N-H⋯O link. This results in infinite sheets lying parallel to (100).

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(E)-N′-[1-(2-Hy­droxy­phen­yl)ethyl­idene]-2-phen­oxy­acetohydrazide–2,2′-(1,1′-azinodiethyl­idyne)diphenol (2/1)

The formula unit of the title mol-ecular complex, 2C(16)H(16)N(2)O(3)·C(16)H(16)N(2)O(2), consists of two (E)-N'-[1-(2-hy-droxy-phen-yl)ethyl-idene]-2-phen-oxy-acetohydrazide mol-ecules and one mol-ecule of 2,2'-(1,1'-azinodiethyl-idyne)diphenol, with the latter located on a crystallographic inversion center. The acetohydrazide mol-ecules are linked into a supermolecular chain along the c axis ...

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عنوان ژورنال:

دوره 66  شماره 

صفحات  -

تاریخ انتشار 2010